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September 22, 2009 *Extraction of Organic Compound Trimyristin* from Nutmeg hire *Recrystal*l*ization* and Simple Distillation Techniques Introduction The general attain of this experiment is to illustrate the extraction of a solid natural product from its natural source by extraction with an ultra solvent. Specifically, we go forth be extracting trymyritsin from nutmeg tree. Trymyritsin is nutmeg’s major triglyceride and accounts for approximately 20-25% of the total dried campaignt of ground nutmeg. By using a combination of recrystallization/reflux and simple distillation techniques, we will extract crystals from a nutmeg and methylene chloride mixture. once we tone down the crystals with dimethyl ketone and dry them through vacuum filtration, we atomic number 50 weigh the crystals to find our percent yield. We r egress out then carry through a MelTemp experiment on the crystallized sample to specialize the dissolve point of trimyristin. Safe ty Info Be sure to theatrical role boiling chips when boiling a liquidness to prevent bumping pulmonary tuberculosis charge when working with diethyl quintessence. Diethyl ether is highly volatile and flammable, do not boil in an open vessel procedure methylene chloride in a well-ventilated area. Avoid breathing blue devils and try to prevent cope with with skin.

Be sure to toil gloves when working with methylene chloride utilisation caution and good brain when working with the estrus place Acetone inhalation, skin contact, and vap or contact with eyes can be very painf! ul so use caution and wear gloves when working with acetone Table of Reagents Procedure In this lab, we will begin by measuring 50 mL of methylene chloride into a receive cylinder and putting it into a 100 mL round-bottom flask. Then measure out 5 g of nutmeg in a tared experience glass. Add the 5 g of nutmeg and a some boiling chips to the round-bottom flask. capture the flask to a capacity and reflux the mixture for 45 minutes by warming the flask with a heating mantle. Position the snorkel...If you want to crap a full essay, lay it on our website: BestEssayCheap.com

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